Synthetic strategies for the application of anodic coupling to the ...

A precipitate formed was filtered, washed with MTBE, and dried under reduced pressure. 1-(2,2-Dimethoxyethyl)cyclobutane-1-carbonitrile (2a). Yield: 91 g, 82% ( ...







An Efficient and Highly Diastereoselective Synthesis of ... - AWS
We here report the preparation of a new 2,6,8-trisubstituted bicyclic tripeptidomimetic scaffold through TFA- mediated cyclization of a linear ...
Synthesis of a novel tripeptidomimetic scaffold and biological ...
General method for the preparation of ?-carbolines (compounds 2, 3, 4, 8, 10). To a solution of tryptophan or tryptophan methyl ester or 2-amino-3-(1H-indol-3- ...
University of Groningen Industrial applications of multiple bond ...
(2,2-dimethoxyethyl)-3-methoxy-O-methyltyrosinamide 15e. This residue was purified by flash chromatography (7:3 hexane/EtOAc) to give 15e (82%) as a white solid.
Synthesis of ?-carboline derivatives - Sciforum
A single intraperitoneal injection (0.6 ml/kg) of dimethoxyethyl phthalate (DMEP) was given to groups of Wistar strain rats on day 10, 11, 12, ...
Experimental Methods - The Royal Society of Chemistry
l'ester boronique 18a synthétisé dans le chapitre 2. Elles ont permis d ... 2-(2,2-Diméthoxyéthyl)-3-((4,4,5,5-tétraméthyl-1,3,2-dioxaborolan-2-yl ...
Thèse de Tiphaine Dedours, Université de Lille, 2020
... ester de carbonate. Cette étape est suivie par l'attaque d'un ... 2-(2,2-diméthoxyéthyl) phényl isonitrile comme isonitrile convertible dans ...
THESE DE DOCTORAT
... 2,2-Dimethoxyethyl)-N,?-dimethylbenzenemethanamine (5m). The title compound was prepared according to GP1 using boronic ester 1 (0.118 g,. 0.508 mmol) and 2,2 ...
Cu-Catalysed Coupling of Aliphatic Amines with Alkylboronic Esters
... 2,2-Dimethoxyethyl)-N,?-dimethylbenzenemethanamine (5m). The title compound was prepared according to GP1 using boronic ester 1 (0.118 g,. 0.508 mmol) and 2,2 ...
Cu-catalyzed coupling of aliphatic amines with alkylboronic esters
The reaction mixture was sampled at the end of the required reaction time and the conversion was determined by HPLC with reference to a 0.05M caffeine solution.
Amidation of Unactivated Ester Derivatives Mediated by ...
3-(2,2-Dimethoxyethyl)-1-tosyl-1H-indole 3p: Prepared according to. General procedure for the preparation of acetals. Starting from methyl 2-(1- tosyl-1H-indol- ...
Hantzsch Esters as Formylation Agents under Photochemical ...
5.5.17 2-(1-Cyclohexyl-2,2-dimethoxyethyl) malononitrile (16a) ...................... 60. 5.5.18 2-(1,1-Dimethoxy-2-phenylpropan-2-yl) malononitrile (17a) ...
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