Development of the Table of Initial Isolation and Protective Action ...
Triethylene glycol monomethyl ether (125 mL, 798 mmol, 1.00 equiv.), methanesulfonyl chloride (65 mL, ... are the parameters that determine the density.
Supporting Information - The Royal Society of ChemistryThe mixture was cooled to 0 °C using an ice/water bath and then methanesulfonyl chloride (0.53 mL, 6.84 mmol, 1.5 equiv.) was added to it dropwise. The ... Total synthesis of the proposed structure of Sclerophytin F and ...methanesulfonyl chloride (0.25 mL, 3.2 mmol) dropwise. The mixture was stirred at ?15 °C for 30 min and the reaction was quenched by the addition of water. Supporting Information - The Royal Society of Chemistrymethanesulfonyl chloride (0.58 mL, 7.5 mmol) followed by the addition of triethyl ... J = 5.0 Hz, 1H), 3.37 (td, J = 5.5, 11.0 Hz, 1H), 2.77 (s, 3H), 2.13 ...
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